Brightstar question.

Discussion in 'Drug Chemistry' started by Amaru, Jul 29, 2008.

  1. Amaru

    Amaru Member

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    The brightstar method seems fairly straightforward in theory.

    What chemicals in that method are surreptitious?

    The saffarole and sassafras oil are closely watched.

    Heres a list of the chemicals provided in brightstar:


    • Safrole (160g)(sassafras oil, yellow camphor oil) (Natural/Essential Oil distributor)
    • Dimethylformamide (DMF) (350mL) (Diethylformamide or Formamide will work)
    • p-Benzoquinone (Quinone, Benzoquinone) (120g) (Photo Shop, or Chem supply)
    • Palladium Chloride (PdCl2) (2g) (Photo Shop, or chem supply)
    • Methylene Chloride (DiChloroMethane, DCM) (this can be distilled from automotive solvents (just go into Nationwise, PepBoys, Sears, AutoZone And read the labels) Or a Liter can be bought from a Chem supplier.)(Zip-Strip furniture polish remover)
    • Hg-salt (1 gram of: HgCl2, Hg(NO3)2, Hg(acetate)2, HgCl, It can be anything, and 1g should last you a long time.)
    • Isopropyl Alcohol (IPA, Pharmacies 91% Isopropyl Alcohol will be available)(get +3L)(don't get the 70% stuff) (or you can get pure stuff from a chem supplier)
    • Epsom Salts (Magnesium Sulphate) (MgSO4) (grocery store/pharmacy) (Spread out on a cookie sheet, and bake in the oven at 200°C for 3hr to dry them - pretty useless if you don't dry it)
    • Thick Al foil (heavy duty, or pie pans from the Grocery store)
    • Muriatic Acid (31.45% HCl)(Pool pH down, Driveway cleaner, ~3$/gallon)
    • Sodium Hydroxide (NaOH) (Drain Cleaner Crystals) (Read these labels, Get the stuff that is JUST NaOH.) (Red Devil Lye, Lye - Hardware Store)
    • Ammonium Chloride (NH4Cl) (Photo Store or Chem Supplier)
    • Paraformaldehyde (Hardware store) (called Mildewcyde or DiGas - made by the same people who brought you Damp-Rid - hint-hint)
    • Peanut oil (this is a high boiling oil that we will use as an oil bath on the hotplate/stirring plate combo)
    • Acetone (for cleaning your glass and crystal work-up) (Paint Section of Hardware Stores)
    • Xylene (for crystallization) (paint section - thinner - get it specifically)

    The first four are the chemicals concerned about. For information purposes.
     
  2. Doctor War

    Doctor War Member

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    The hardest one for you otog et will be the palladium - It's expensive, a listed precrusor, and comparatively difficult to improvise. benzoquinone is ridiculously easy; it's one of the two components used in developing fluid. Safrole? Distill from any number of essential oils. Formamide will need to be picked up from a chemical supply house, but if you get anything less then 99% purity, you'll turn out the dreaded red tar.

    Mercury salt will be hard to buy, but is simple to make if you CBF.
     
  3. polymer

    polymer Senior Member

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    palladium is a catalyst, and a rare metal... safrole needs to be isomerized to isosafrole via catalytic hydrogenation, this is done with palladium. it is indeed expensive, and likely watched
     
  4. LSDMIKE

    LSDMIKE Member

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    Mercury shit i hope you know what your doing
    there is methods out there that you don't need this shit..palladium is a catalyst
    and if you don't have it you need to make it yourself very big hard job
     
  5. Doctor War

    Doctor War Member

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    Mercury's a fucking cakewalk.
     

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