How to make acid (im not asking.... i have the answer)

Discussion in 'LSD - Acid Trips' started by Zen_Master3568, Mar 14, 2008.

  1. ESRUOS ENO

    ESRUOS ENO Senior Member

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    IDK... Why havent you tried this to find out...eh?
     
  2. undercooked

    undercooked Member

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    I'm no chemist, but I don't believe these directions at all. They don't seem very precise. e.g. they say to "simmer" something instead of giving a temperature. But that is a little bit irrelevant when these instructions are probably fake anyway. If it were this easy to make lsd and as easy to extract ergotamine tartrate from some over the counter drug as you think it is, then I suspect people would have been doing it long before you much more commonly than they do in reality.

    I thought that I would search for some related terms on google.com/scholar to see if there were any articles that came up which could at least give some idea of the process involved in making lsd. I found this patent from 1985 (Process for the production of ergotamine alkoloids - Patent 4492664) dealing with some of the initial steps that could be taken to create a precursor to lsd, and it sounds like a much more complicated process than the one you've shared. LSD is a pretty sensitive chemical. After all, the end product degrades when exposed to light or oxygen, so I can only imagine what measures have to be taken with the chemicals involved. For example, the patent writes that parts of the process have to be done under argon or another inert gas.

    Maybe you should get a little more chemistry experience first.
     
    1 person likes this.
  3. Squilla

    Squilla Banned

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    LOL:

    "If it were this easy to make lsd and as easy to extract ergotamine tartrate from some over the counter drug as you think it is, then I suspect people would have been doing it long before you much more commonly than they do in reality."

    Take a walk outside, it is that easy, and there are people making it everywhere.
     
  4. Beckner420

    Beckner420 troll

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    I dont think LSD is as hard to make as people say it is, but its probably not easy either.

    Squilla... your on crack.
     
  5. HauntedGraffiti

    HauntedGraffiti Member

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    its not amazingly hard, just the materials to get them are extremely hard to get, unless your a college proffesor or have a special chemical license. theres different ways to make LSD, and most of them require a lab, and a year or two in a chemestry class.
     
  6. undercooked

    undercooked Member

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    Because people just advertise it in the streets when they manufacture LSD? I'm sure you know all about it. Maybe it is different where you live, but I still don't believe you.

    Wouldn't there be more reports of people being arrested for manufacturing LSD? Moreover, active dosages of LSD are so minute that if one were capable of producing LSD, he or she could probably produce such a vast quantity that there would be no need to continuously produce it. I doubt that it would take more than a handful of people to create enough LSD to supply everyone in the world who wants any if not a single person; this is the only reason that acid was as ever as popular as it is because I'd bet the farm that it's a whole lot more difficult to make than you say it is.

    Also, nobody has provided any credible sources to support anything discussed in this thread. I find that reason enough to be sceptical. Never trust the internet.
     
  7. undercooked

    undercooked Member

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    I was reading about LSD synthesis on another forum and came across this. However, I can not attest to its legitimacy. It's said that this is a total synthesis and that there are easier ways to do it.

     
  8. Fancyabongripski420

    Fancyabongripski420 Member

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    yeah how good does it come out???
     
  9. cabby

    cabby Member

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    mineapolis huh? im down here in austin. u have many sources up there or what cause down here there isnt shit
     
  10. Psychedelic94

    Psychedelic94 Member

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    There is more than one way to make acid - here's another way - buy the book Acid Trips and Chemistry by Cam Cloud - very detailed and reasonably understandable.
     
  11. Sitar

    Sitar Member

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    You could just spray some WD 40 on rye bread then sprinkle baking soda on it. Stick it in the back of your fridge, wait until it molds then eat around the mold.
    Thats my way though it is not very safe.
     
  12. woodlouse

    woodlouse Member

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    This only works with WD41 manufactured in N. Korea.
     
  13. Cerveau

    Cerveau Member

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    Why does this keep coming up? We're all reasonable adults. Let's use our powers of deducive reasoning to figure out if its relatively easy to make acid.

    If acid was relatively easy to make, those with relative intelligence would be able to make it, provided the right equipment and tools were/are availabe, right? So how can we tell it isn't?

    Because not everyone is making acid. It should be that simple. I don't think anyone in this thread could get there hands on half the ingredients. Maybe some can, but the simple fact of the matter is you need sterilized equipment and a lab. You can't just simmer. This isn't home ec.

    Jesus, move on already.

    Not to mention you can post all sorts of shit from any site you want and you'd still be making acid out of Beck's beer.

    Here's the recipe I found and I found it on matrese.com.

    How's that for siting my source.

    [All text used without permission
    from the "Whole Drug Manufacturers Catalog"
    Any typos are YOUR problem
    For informational purposes only
    I take NO responsibility for YOUR actions
    Be careful --Ed.]



    NOTE: the techniques described herein are potentially dangerous. It
    is highly recommended that the physical and chemical properties of
    the reagents used and the reactions employed be given further study
    by persons unfamiliar with them. For the layman to attempt these
    procedures without first thoroughly preparing himself is to invite
    almost certain disaster. The publishers therefore disclaim
    responsibility for any damage or injury resulting from the improper
    handling of the chemicals and techniques described, and strongly
    urge all persons unqualified to perform the reactions to use
    extraction rather than synthesis.



    #1: Kitchen chemistry

    Extraction of LSA (Lysergic acid amide)
    from Morning Glory (Ipomosea Purpurea) seeds
    or Hawaiian Baby Wood Rose (Argyreia Nervosa) seeds


    NOTE: Morning Glory seeds may be coated with a toxic chemical by
    the seed company in order to prevent ingestion. If a packet of
    seeds contains coated seeds this fact should be stated on the
    container. Soaking the seeds in warm water for 1/2 hour and
    rinsing in a strainer should remove this coating.

    NOTE: while many varieties of morning glory contain the active LSA
    (Lysergic acid amide), the yield varies greatly. Therefore, use
    only Pearly Gates, Wedding Bells, and Heavenly Blue varieties for
    best results.


    Kitchen chemistry follows.


    Materials: blender, funnel, filter paper, petroleum ether or
    lighter fluid, methanol (wood alcohol), glass jar,
    Pyrex baking dish


    Grind Morning Glory or Hawaiian Baby Wood Rose seeds in a
    blender until they are a fine powder, and spread them out to
    dry.
    Soak the powder with lighter fluid or petroleum ether. Cap
    the container to avoid fumes, and don't smoke nearby, or
    you'll be very sorry.

    In a well-ventilated area (neither ether nor lighter fluid are
    good for you), filter the solution through filter paper in a
    funnel. Discard the filtrate (the liquid).

    Dry mash completely.

    Soak mash in methanol (wood alcohol) for 2 days. Be careful
    -
    its vapors are poisonous and may be explosive.

    Filter, and save the filtrate.

    Soak the mash in methanol again a further 2 days.

    Filter. Discard the mash, save the filtrate.

    Pour both filtrates into a large, flat dish and evaporate in
    the absence of direct sunlight. Sunlight will break down the
    LSA. Preferably, perform ALL procedures in a cool, well-
    ventilated place away from sunlight.

    After evaporation, a yellow gum will remain in the dish.
    Scrape it up.

    To dose on the LSA, add some harmless filler (starch, flour,
    milk sugar) to the gum until it is not sticky. Put in gelatin
    capsules or take as is. 30 g Morning Glory seeds or 15
    Hawaiian Baby Woodrose seeds should make a goodly trip, so
    adjust dosage accordingly.

    If you want to turn LSA into LSD, you can [see below], but
    it's MUCH more difficult and VERY unsafe.




    #2: Extraction of Lysergic Acid Amides


    Start with domestic Morning Glory seeds, the young seeds of
    the Hawaiian Baby Wood Rose, cultured ergot or naturally
    occurring ergot compounds.


    NOTE: Morning Glory seeds may be coated with a toxic chemical by
    the seed company in order to prevent ingestion. If a packet of
    seeds contains coated seeds this fact should be stated on the
    container. Soaking the seeds in warm water for 1/2 hour and
    rinsing in a strainer should remove this coating.

    NOTE: while many varieties of morning glory contain the active LSA
    (Lysergic acid amide), the yield varies greatly. Therefore, use
    only Pearly Gates, Wedding Bells, and Heavenly Blue varieties for
    best results.


    Reduce seed material to a fine powder in a blender, and spread
    it out to dry. Grind again if not fine enough after the first
    time due to dampness.

    Saturate powdered seed material with lighter fluid, naphtha or
    ligroine. When completely saturated, it should have the
    consistency of soup.

    Pour into a chromatography column and let it sit overnight.

    Remove the fatty oils from the material by dripping the
    solvent through the column slowly, and testing the liquid that
    comes through for fats by evaporating a drop on clean glass
    until it leaves no greasy film. (It should take several
    ounces of solvent for each ounce of seeds).

    Mix 9 volumes of chloroform with 1 volume of concentrated
    ammonium hydroxide and shake in a separatory funnel. When it
    settles, the chloroform layer will be on the bottom. Drain
    the chloroform layer and discard the top layer.

    Drip the chloroform wash through the column and save the
    extract. test continuously by evaporating a drop on clean
    glass until it ceases to fluoresce.

    [It is NOT explicit in the source, but if extracting
    from ergot, I would start with the ergot alkaloid base at
    this point. --Ed.]

    Evaporate the chloroform extracts, and dissolve the residue in
    the minimum amount of a 3% tartaric acid solution. If all the
    residue doesn't dissolve, place it into suspension by shaking
    vigorously.

    Color the solution with an acid base indicator, and titrate to
    find the approximate number of moles of the alkaloid present.

    Transfer the solution to a separatory funnel, and wash the
    other vessel with acid in order to get all the alkaloid out.
    Pour the washings in the funnel also.

    Bring the pH up to make the solution basic by adding sodium
    bicarbonate solution, and add an equal volume of chloroform.

    Shake thoroughly, let it settle, remove the bottom layer and
    set aside.
    Again add an equal portion of chloroform, shake, let settle
    and remove bottom layer.

    Combine chloroform extracts (bottom layers) and evaporate.

    The residue remaining after evaporation is a semi-pure
    concentrate of LSA (lysergic acid amide). The amide requires
    some experimentation for dosage, but 1 mg of the concentrate
    is a reasonable starting point. 1 mg LSA will produce effects
    comparable to 100 micrograms of LSD.




    #3: Ergot culture


    NOTE: contact with ergot compounds can be dangerous. Only after a
    basic understanding of the techniques employed in the handling of
    dangerous or poisonous organisms is reached should one proceed with
    the culture of ergot.

    The need for absolute sterility cannot be overstressed. Consult
    any elementary text on bacteriology for the correct equipment and
    procedures. Avoid prolonged contact with ergot compounds, as they
    are poisonous and can be fatal.


    A) Get a source for Claviceps Purpurea fungus


    If no source can be found, you can make a field trip to obtain
    it from rye or other cereal grasses. Rye grass is the best
    choice. The ergot will appear as a blackish growth on the
    tops of the rye where the seeds are. They are approximately
    the same shape as the seeds and are referred to as "heads" or
    "ergot". From these heads or ergot sprout the Claviceps
    Purpurea fungi.

    They have long stems and bulbous heads when viewed under a
    strong glass or microscope. It is these that must be removed
    from the ergot, free from contamination, and used to inoculate
    the culture material.


    B) Make a culture medium


    Combine the following ingredients in about 500 ml distilled
    water in a 2 L small-neck flask:


    Sucrose 100 g

    Chick pea meal 50 g
    Calcium nitrate 1 g
    Ca(NO3)2
    Monopotassium phosphate 0.25 g
    KH2PO4
    Magnesium sulphate 0.25 g
    MgSO4
    Potassium chloride 0.125 g
    KCl
    Ferrous sulphate heptahydrate 8.34 mg
    FeSO47H20
    Zinc sulphate heptahydrate 3.44 mg
    ZnSO47H20


    Add water to make up one liter

    Adjust to pH 4 with ammonia solution and citric acid

    Sterilize by autoclaving


    C) Make a culture


    Inoculate the sterilized medium with Claviceps Purpurea under
    sterile conditions, stopper with sterilized cotton and
    incubate for two weeks, periodically testing and maintaining
    pH 4. After two weeks a surface culture can be seen on the
    medium. Large-scale production of the fungus can now begin.


    D) Large-scale production


    Obtain several ordinary 1 gallon jugs.

    Place a two-hole stopper in the necks of the jugs.

    Fit a short (6 inch) tube in one hole, leaving two inches
    above the stopper. Fit a short rubber tube to this. Fill a
    small (500 ml) Erlenmeyer flask with a dilute solution of
    sodium hypochlorite (NaClO). Extend a glass tube from the
    rubber so the end is immersed in the hypochlorite.

    Fit a long glass tube in the other stopper hole. It must
    reach near the bottom of the jug and have about two inches
    showing above the stopper. Attach a rubber tube to the glass
    tube and fit a short glass tube to the end of the rubber tube.


    Fill a large glass tube (1" x 6") with sterile cotton and fit
    one-hole stoppers in the ends. Fit the small glass tube in
    the end of the rubber tube into one stopper of the large tube.
    Fit another small glass tube into the other stopper. A rubber
    tube is connected to this and attached to small air pump
    (obtained from a tropical fish store).

    With this aeration equipment you can assure a supply of clean
    air to the Claviceps Purpurea fungus while maintaining a
    sterile environment inside the solution.

    Dismantle the aerators. Place all the glass tubes, rubber
    tubes, stoppers and cotton in a paper bag, seal tightly with
    wire staples and sterilize in an autoclave.

    Fill the 1-gallon jugs 2/3 to 3/4 full with the culture medium
    and autoclave.

    While these things are being sterilized, homogenize in a
    blender the culture already obtained and use it to inoculate
    the material in the gallon jugs. The blender must be sterile.


    EVERYTHING must be sterile.


    Assemble the aerators. Start the pumps. A slow bubbling in
    each jug will provide enough oxygen to the cultures. A single
    pump may be connected to several filters.

    Let everything sit at room temperature (25 C) in a dark place
    (never expose ergot alkaloids to bright light - they will
    decompose) for a period of ten days.

    After ten days, adjust the culture to 1% ethanol using 95%
    ethanol under sterile conditions. Maintain growth for another
    two weeks.


    E) Extract ergot alkaloids


    After a total of 24 days growth period, the culture should be
    considered mature. Make the culture acidic with tartaric acid
    and homogenize in a blender for one hour.

    Adjust to pH 9 with ammonium hydroxide and extract with
    benzene or chloroform/iso-butanol mixture.

    Extract again with alcoholic tartaric acid and evaporate in a
    vacuum to dryness.

    The dry material is the salt (the tartaric acid salt, the
    tartrate) of the ergot alkaloids, and is stored in this form
    because the free basic material is too unstable and decomposes
    readily in the presence of light, heat, moisture, and air.

    To recover the free base for extraction of the amide or
    synthesis to LSD, make the tartrate basic with ammonia to pH
    9, extract with chloroform, and evaporate in vacuo.





    #4: Synthesis of LSD from ergot alkaloids or LSA

    (including sections on isomerization, separation,
    purification & crystallization)


    NOTE: the chemicals and reactions described below are potentially
    dangerous even to an organic chemist in a well-equipped laboratory.

    The publishers therefore disclaim responsibility for any damage or
    injury resulting from the improper handling of the chemicals and
    techniques described, and strongly urge all persons unqualified to
    perform the reactions to use instead the comparatively easier,
    safer ergot culture and LSA extraction process.


    A) Synthesis of LSD
    (iso- & dextro-lysergic acid diethylamide)


    PREPARATORY: obtain one red and one yellow photographic safety
    light and one weak, long-wave ultraviolet light. These are used to
    prevent the hydrolysis of lysergic acid compounds.

    NOTE: Aluminum foil must be used to cover the chemicals when light
    is present. Rubber gloves must be worn; these compounds are
    extremely poisonous.

    [The source implies but does not state that one may replace
    "ergot alkaloid" in the following with the seed-derived semi-
    pure LSA concentrate from #2. --Ed.]


    USING YELLOW LIGHT:

    Place one volume of ergot alkaloid in a small roundbottom
    flask. Add 2 volumes of anhydrous hydrazine and reflux for 30
    minutes, or the mixture may be heated in a sealed tube at 112
    Celsius for 30 minutes. If the reflux technique is used,
    maintain atmospheric pressure by using an open container or
    fractionating column.

    After heating/refluxing, add 1.5 volumes of water to the
    mixture and boil gently for 15 minutes. After boiling is
    complete, cool the mixture in a refrigerator until
    solidification. The solid material obtained is iso-lysergic
    acid hydrazide.

    USING RED LIGHT:

    Chill all chemicals (reagents) to be used to 0 Celsius. Place
    an open flask in an ice bath. Add 100 ml concentrated
    hydrochloric acid (chilled to 0 C).

    Quickly add 2.82 g of the lysergic acid hydrazide to the
    hydrochloric acid, being careful to maintain a temperature of
    0 Celsius.

    Add 100 ml of a 0.1 N (1/10th Normal) solution of sodium
    nitrite (chilled to 0 C) and stir vigorously for 3 minutes.

    Continue stirring at 0 Celsius and add dropwise 130 ml of the
    hydrochloric acid.

    When the acid addition is complete, continue stirring for 5
    minutes, then neutralize the solution with sodium bicarbonate,
    using a saturated water solution of the bicarbonate.

    Extract the solution with ether, remove the water layer, and
    dissolve the gummy substance in ether. Add this to the ether
    layer.

    Add 3 g of diethylamine for every 30 ml of the ether extract.

    Let this stand in the dark, and gradually warm up to 20
    Celsius for at least 24 hours.

    Evaporate this solution in a vacuum.

    The material remaining is a mixture of the inactive
    iso-lysergic acid diethylamide and the active lysergic acid
    diethylamide (LSD-25). The inactive isomer must now be
    converted (isomerized) to the active isomer to greatly
    increase the yield, since the inactive compound predominates
    in this synthesis.



    B) Isomerization of iso-LSD into the active LSD-25


    USING THE RED LIGHT:

    Dissolve the synthesized material into the minimum amount of
    ethyl alcohol.

    Mix a 4 Normal solution of potassium hydroxide in ethanol.
    The amount of solution needed is twice the volume of the
    iso-LSD/ethanol solution.

    Add the two solutions together and let the mixture sit for 4
    hours at room temperature.

    Neutralize the mixture with dilute hydrochloric acid, then
    make it slightly basic with ammonium hydroxide.

    Extract the mixture with chloroform, sparate the chloroform
    layer, and extract this four times with a 25% volume of water.

    Evaporate the chloroform in a vacuum. Discard the water
    extracts. The material left after evaporation a mixture of
    iso-LSD and LSD-25, the active LSD predominating.

    The mixture may now be separated by chromatography and the
    iso-LSD again isomerized by the above process.



    C) Separation, purification & crystallization of LSD-25


    USING A DARKROOM:

    The material obtained from the isomerization process is now
    dissolved in a solution prepared from 3 parts benzene/1 part
    chloroform. Use 50 ml solvent per 1 gram LSD material.

    Mix a slurry basic alumina in benzene. Pack it into a 1 inch
    chromatoghraphy column until it fills 6 inches.

    When the slurry settles, drain the benzene/chloroform down to
    the level of the basic alumina, and carefully add an equal
    amount of the LSD/solvent solution.


    USING A WEAK, LONG-WAVE ULTRAVIOLET LIGHT:
    (to follow the blue band only)

    Drain the solution through the column. The fastest-moving,
    blue fluorescent band contains the LSD-25. Collect this
    fraction and evaporate in a vacuum. The syrup remaining will
    crystallize spontaneously, but slowly. Do not heat.

    Use the UV light only whe necessary to follow the blue band in
    order to avoid decomposition of the compounds.

    Dissolve the syrup or crystal in tartaric acid solution and
    recrystallize to form the stable end-product (dextro lysergic
    acid diethylamide tartrate).

    The material remaining in the column may be removed with
    methanol, evaporated in a vacuum, and recycled through the
    isomerization and subsequent procedures by itself or combined
    with fresh material.
    Also, all leftover solutions and residues may be neutralized
    with socium bicarbonate, evaporated in vacuo, and extracted
    with ammoniacal chloroform, the extract evaporated to dryness,
    and the residue reused.
     
  14. Cerveau

    Cerveau Member

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    #5: Preparation of lysergic acid from the amide





    NOTE: this synthesis is as difficult and dangerous as the rest, and

    is of use only if using one of the following two LSD synthesis

    methods, which require lysergic acid as the starting compound. The

    lysergic acid amide obtained from the extract of ergot or seeds

    need not be converted to the acid prior to its use in the synthesis

    of LSD providing that the synthesis used is #4 given above, and

    giving the starting material "ergot alkaloid".





    Dissolve 10 g lysergic acid amide in 200 ml methanolic

    potassium hydroxide solution.



    Remove the methanol by vacuum as soon as the amide is

    dissolved.



    Dissolve the residue which is left into 200 ml of an 8%

    solution of potassium hydroxide in water.



    Heat this mixture on a steam bath for 1 hour.



    Pass a steam of nitrogen gas through the flask during the

    heating process. (The ammonia which is evolved in the gas

    stream may be titrated with hydrochloric acid in order to

    follow the reaction.)



    Neutralize the mixture with tartaric acid (neutral to congo

    red) and run it through a filter paper.



    Extract the mixture with ether in a separatory funnel. Save

    the water layer, discard the ether layer.



    Filter the solution through a filter paper and evaporate.



    Upon evaporation, dry crystals of lysergic acid will be

    obtained.









    #6: Synthesis of LSD

    using lysergic acid

    the quickest way to make pure LSD-25

    PREPARATORY: see #4



    NOTE: The chemicals and techniques described are potentially

    dangerous. It is highly recommended that the physical and chemical

    properties of the reagents used be studied by those persons

    unfamiliar with them before the synthesis is attempted.







    USING THE YELLOW LIGHT:



    5.36 g of d-lysergic acid are suspended in 125 ml

    acetonitrile, and the suspension is cooled to about -20

    Celsius in a bath of acetone cooled with dry ice.



    To the suspension is added a cold (-20 C) solution of 8.82 g

    of trifluoracetic anhydride in 75 ml acetonitrile. The

    mixture is allowed to stand at -20 C for about 1 1/2 (one and

    one-half) hours.



    (During this time the suspended material dissolves and the

    d-lysergic acid id converted to the mixed anhydride of

    lysergic and trifluoracetic acids.)



    The mixed anhydride can be separated in the form of an oil by

    evaporating the solvent in vacuo at a temperature below about

    0 Celsius.



    Everything must be kept anhydrous.





    USING THE RED LIGHT:



    The solution of mixed anhydrides in acetonitrile from above is

    added to 150 ml of acetonitrile containing 7.6 g of

    diethylamine.



    The mixture is held in the dark at room temperature for about

    2 hours.



    The acetonitrile is evaporated in vacuo, leaving a residue of

    LSD-25 plus impurities.



    The residue is dissolved in 150 ml of chloroform and 20 ml of

    ice water.



    The chloroform layer is removed and the aqueous layer is

    extracted with several portions of chloroform. The chloroform

    portions are are combined and, in turn, washed with four 50 ml

    portions of ice-cold water.



    The chloroform solution is then dried over anhydrous sodium

    sulfate and evaporated in vacuo.



    NOTE: following the completion of this synthesis, follow the

    procedures described for separation, purification, and

    crystallization of LSD-25. If a higher yield is desired, follow

    the procedure on isomerization after doing the separation,

    purification, and crystallization.









    #7: Synthesis of LSD

    using lysergic acid

    high-yielding and fast





    PREPARATORY: see #4



    NOTE: The chemicals and techniques described are potentially

    dangerous. It is highly recommended that the physical and chemical

    properties of the reagents used be studied by those persons

    unfamiliar with them before the synthesis is attempted.



    NOTE: the following procedure gives good yield and is very fast,

    with little iso-lysergic acid being produced. However, the

    stoichiometry must be exact or yields will drop





    USING WHITE LIGHT:



    Sulfur trioxide is produced in an anhydrous state by carefully

    decomposing anhydrous ferric sulfate at approximately 480

    Celsius. Store under anhydrous conditions.



    USING WHITE LIGHT:



    A carefully-dried 22 liter RB flask fitted with an ice bath,

    dropping funnel, and mechanical stirrer is charged with 10 to

    11 liters of dimethylformamide (freshly distilled under

    reduced pressure).



    The condenser and dropping funnel are both protected against

    atmospheric moisture.



    2 lb. of sulfur trioxide (Sulfan B) are introduced dropwise,

    very cautiously with stirring, during 4 to 5 hours. The

    temperature is kept at 0-5 Celsius throughout the addition.



    After the addition is complete, the mixture is stirred for 1

    to 2 hours until some separated crystalline sulfur trioxide-

    dimethylformamide complex has dissolved.



    The reagent is transferred to an air-tight automatic pipette

    for convenient dispensing, and kept in the cold. Although the

    reagent, which is colorless, may change to yellow and red, its

    efficiency remains unimpaired for three to four months in cold

    storage.



    An aliquot is dissolved in water and titrated with standard

    NaOH to a phenolphthalein end point.





    USING RED LIGHT:



    A solution of 7.15 g of d-lysergic acid monohydrate (25 mmol)

    and 1.06 g of lithium hydroxide hydrate (25 mmol) in 200 L of

    MeOH is prepared.



    The solvent is distilled on the steam bath under reduced

    pressure.



    The residue of glass-like lithium lysergate is dissolved in

    400 ml of anhydrous dimethyl formamide.



    From this solution, about 200 ml of the dimethyl formamide is

    distilled off at 15mm pressure through a 12-inch helices

    packed column.



    The resulting anhydrous solution of lithium lysergate left

    behind is cooled to 0 Celsius and, with stirring, treated

    rapidly with 500 ml of SO3DMF solution (1.00 Molar).



    The mixture is stirred in the cold for 10 minutes and then

    9.14 g (125.0 mmol) of diethylamine is added.



    The stirring and cooling are continued for 10 minutes longer,

    when 400 ml of water is added to decompose the reaction

    complex.



    After mixing thoroughly, 200 ml of saturated aqueous saline

    solution is added. The amide product is isolated by repeated

    extraction with 500 ml portions of ethylene dichloride.



    The combined extract is dried and then concentrated to a syrup

    under reduced pressure. Do not heat the syrup during

    concentration. The LSD may crystallize out, but the crystals

    and the mother liquor may be chromatographed according to the

    instructions in the synthesis of LSD #4.





    kk, now if you understand ALL of that... then MAYBE you can give it a shot.
     
  15. Squilla

    Squilla Banned

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    Consider it copy and pasted :D

    I intend on making LSD....someday....
     
  16. Nivekian

    Nivekian Member

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    It sure used to be... I used to be able to buy it at $0.60 a hit, now people are asking upwards to $10 a hit... With prices that high I'd rather go pick a mushroom!
     
  17. ImaMuffin

    ImaMuffin Member

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    I googled all the chemicals on google shopping... they are ALL for sale!

    however.. if i actually bought them, I'm willing to bet the dea would throw me in jail the next day.
     
  18. rayoflight110

    rayoflight110 Member

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    life is beautiful
     
  19. .Xen.

    .Xen. Member

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    thats why you have friends with credit cards... have every chemical bought from a different account and sent to a different address.. i know i have at least 14 friends that would be willing to help me get the shit to make acid... were i to do it... i mean i have a lot more chem before i could even think of doing it..

    also, you guys know that there is a VERY detailed recipe on how to synthesize LSD in Alexander Shulgans book TiKAL.. along with the synthesis for DMT AMT 5-meo-DMT 5-meo-DiPT ect. there like 200 chemicals in it... same with his first book PiKAL, which is all about phenethlamines. :) I <3 Phenethlamines. lol, oh and on top of that you can have them ordered to your nearset Borders book store for free and then go screen them... i did, and they look amazing but i didnt have the money before... lol. there like 25.00 a piece or something.
     
  20. hawaiiankine

    hawaiiankine Senior Member

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    I can see why this is the most viewed thread.

    Loved it!

    aloooha!
     

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